سال انتشار: ۱۳۸۶

محل انتشار: پانزدهمین همایش انجمن بلورشناسی و کانی شناسی ایران

تعداد صفحات: ۴

نویسنده(ها):

Ali. R Rezvani – Department of Chemistry, University of Sistan and Baluchestan,P. O. Box 98135-674, Zahedan, Iran
Hassan Hadadzadeh – Department of Chemistry, Isfahan University of Technology, Isfahan 84156-83111, Iran
Hadi Esfandiaria – Department of Chemistry, Isfahan University of Technology, Isfahan 84156-83111, Iran

چکیده:

The new dipicolinate complex of nickel, [Ni(phen) (dipic)H2O].4H2O has been prepared where dipic is dipicolinate or pyridine- 2,6-dicarboxylate and phen is1,10phenanthroline. The crystal structure was determined by single-crystal X-ray diffraction. This complex crystallized in the triclinic system, with space group Pī, a=7.9131(4)Å, b= 10.6006(6) Å, c=13.2268(7) Å, β= ۹۶٫۱۵۸(۱)°, V= 1027.55(10) Å۳, Z= 2. The final R value is 0.0340 for 4677 measured reflections.